Volume 41 Issue 2
Feb.  2026
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ZHANG Shenyu, WANG Rongqiao, LYU Zhengzhe, et al. Evolution of microstructure and elastic modulus of EB-PVD thermal barrier coating induced by sintering[J]. Journal of Aerospace Power, 2026, 41(2):20240398 doi: 10.13224/j.cnki.jasp.20240398
Citation: ZHANG Shenyu, WANG Rongqiao, LYU Zhengzhe, et al. Evolution of microstructure and elastic modulus of EB-PVD thermal barrier coating induced by sintering[J]. Journal of Aerospace Power, 2026, 41(2):20240398 doi: 10.13224/j.cnki.jasp.20240398

Evolution of microstructure and elastic modulus of EB-PVD thermal barrier coating induced by sintering

doi: 10.13224/j.cnki.jasp.20240398
  • Received Date: 2024-06-19
    Available Online: 2025-11-07
  • The microstructure and elastic modulus evolution of electron beam-physical vapor deposition (EB-PVD) thermal barrier coating were studied. The sintering test of EB-PVD thermal barrier coating at 1150 ℃ was carried out, and the microstructure of the test piece after sintering was observed by scanning electron microscope (SEM), and the evolution of columnar crystal gap in ceramic layer was obtained. The elastic modulus of ceramic layer was measured by nanoindenter. The results showed that the elastic modulus of ceramic layer increased rapidly at the initial stage of sintering and then became stable. In order to relate the elastic modulus of ceramic layer with the micro-structure evolution, a simplified cylindrical crystal model of ceramic layer was established based on the prepared microstructure, and the evolution law of the elastic modulus was obtained by using the sintering model based on the microstructure evolution. The results showed that the microstructure evolution induced by sintering led to the change of elastic modulus of ceramic layer. The sintering model based on the microstructure evolution can accurately predict the evolution law of elastic modulus with sintering time, and the error between the measured value and the calculated value was less than ±20%.

     

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  • [1]
    PADTURE N P, GELL M, JORDAN E H. Thermal barrier coatings for gas-turbine engine applications[J]. Science, 2002, 296(5566): 280-284. doi: 10.1126/science.1068609
    [2]
    EVANS A G, MUMM D R, HUTCHINSON J W, et al. Mechanisms controlling the durability of thermal barrier coatings[J]. Progress in Materials Science, 2001, 46(5): 505-553. doi: 10.1016/S0079-6425(00)00020-7
    [3]
    郭洪波, 宫声凯, 徐惠彬. 先进航空发动机热障涂层技术研究进展[J]. 中国材料进展, 2009, 28(增刊2): 18-26. GUO Hongbo, GONG Shengkai, XU Huibin. Progress in thermal barrier coatings for advanced aeroengines[J]. Materials China, 2009, 28(Suppl. 2): 18-26. (in Chinese

    GUO Hongbo, GONG Shengkai, XU Huibin. Progress in thermal barrier coatings for advanced aeroengines[J]. Materials China, 2009, 28(Suppl. 2): 18-26. (in Chinese)
    [4]
    吕伯文, 江鹏, 李定骏, 等. 重型燃气轮机高温叶片热障涂层烧结问题研究进展[J]. 中国材料进展, 2020, 39(11): 855-870. LV Bowen, JIANG Peng, LI Dingjun, et al. Advances on the sintering of thermal barrier coatings for high temperature blade of industrial gas turbines[J]. Materials China, 2020, 39(11): 855-870. (in Chinese

    LV Bowen, JIANG Peng, LI Dingjun, et al. Advances on the sintering of thermal barrier coatings for high temperature blade of industrial gas turbines[J]. Materials China, 2020, 39(11): 855-870. (in Chinese)
    [5]
    陈炳贻. 航空发动机用热障涂层的发展[J]. 材料保护, 1997, 30(2): 19-21. CHEN Bingyi. Development of thermal barrier coatings for aeroengines[J]. Materials Protection, 1997, 30(2): 19-21. (in Chinese

    CHEN Bingyi. Development of thermal barrier coatings for aeroengines[J]. Materials Protection, 1997, 30(2): 19-21. (in Chinese)
    [6]
    ZHAO X, WANG X, XIAO P. Sintering and failure behaviour of EB-PVD thermal barrier coating after isothermal treatment[J]. Surface and Coatings Technology, 2006, 200(20/21): 5946-5955.
    [7]
    THOMPSON J A, CLYNE T W. The effect of heat treatment on the stiffness of zirconia top Coats in plasma-sprayed TBCs[J]. Acta Materialia, 2001, 49(9): 1565-1575. doi: 10.1016/S1359-6454(01)00065-9
    [8]
    ZHANG B C, CHEN Kuiying, BADDOUR N, et al. Failure and life evaluation of EB-PVD thermal barrier coatings using temperature-process-dependent model parameters[J]. Corrosion Science, 2019, 156: 1-9. doi: 10.1016/j.corsci.2019.04.020
    [9]
    张勇. 1 200 ℃烧结EB-PVD YSZ涂层微结构演变的TEM表征与分析[D]. 湘潭: 湘潭大学, 2015. ZHANG Yong. TEM characterization and analysis of microstructure evolution of EB-PVD YSZ coating sintered at 1 200 ℃[D]. Xiangtan: Xiangtan University, 2015. (in Chinese

    ZHANG Yong. TEM characterization and analysis of microstructure evolution of EB-PVD YSZ coating sintered at 1 200 ℃[D]. Xiangtan: Xiangtan University, 2015. (in Chinese)
    [10]
    OLIVER W C, PHARR G M. An improved technique for determining hardness and elastic modulus using load and displacement sensing indentation experiments[J]. Journal of Materials Research, 1992, 7(6): 1564-1583. doi: 10.1557/JMR.1992.1564
    [11]
    CERNUSCHI F, BISON P G, MARINETTI S, et al. Thermophysical, mechanical and microstructural characterization of aged free-standing plasma-sprayed zirconia coatings[J]. Acta Materialia, 2008, 56(16): 4477-4488. doi: 10.1016/j.actamat.2008.04.067
    [12]
    LV Bowen, FAN Xueling, LI Dingjun, et al. Towards enhanced sintering resistance: Air-plasma-sprayed thermal barrier coating system with porosity gradient[J]. Journal of the European Ceramic Society, 2018, 38(4): 1946-1956. doi: 10.1016/j.jeurceramsoc.2017.12.008
    [13]
    KUMAR S, COCKS A C F. Computational modelling of constrained sintering in EB-PVD thermal barrier coatings[J]. Modelling and Simulation in Materials Science and Engineering, 2013, 21(6): 065008. doi: 10.1088/0965-0393/21/6/065008
    [14]
    PARHAMI F, MCMEEKING R M, COCKS A C F, et al. A model for the sintering and coarsening of rows of spherical particles[J]. Mechanics of Materials, 1999, 31(1): 43-61. doi: 10.1016/S0167-6636(98)00049-0
    [15]
    李庆扬. 数值分析[M]. 4版. 北京: 清华大学出版社, 2001.
    [16]
    王志刚, 刘仍谦, 谢敏, 等. Sc2O3和Y2O3复合掺杂ZrO2热障涂层陶瓷材料的组织结构与力学性能[J]. 材料工程, 2024, 52(6): 139-146. WANG Zhigang, LIU Rengqian, XIE Min, et al. Microstructure and mechanical properties of ZrO2 thermal barrier coating ceramic materials doped with Sc2O3 and Y2O3[J]. Journal of Materials Engineering, 2024, 52(6): 139-146. (in Chinese

    WANG Zhigang, LIU Rengqian, XIE Min, et al. Microstructure and mechanical properties of ZrO2 thermal barrier coating ceramic materials doped with Sc2O3 and Y2O3[J]. Journal of Materials Engineering, 2024, 52(6): 139-146. (in Chinese)
    [17]
    FLECK N A, COCKS A C F. A multi-scale constitutive model for the sintering of an air-plasma-sprayed thermal barrier coating, and its response under hot isostatic pressing[J]. Journal of the Mechanics and Physics of Solids, 2009, 57(4): 689-705. doi: 10.1016/j.jmps.2009.01.001
    [18]
    CIPITRIA A, GOLOSNOY I O, CLYNE T W. A sintering model for plasma-sprayed zirconia TBCs Part I: free-standing coatings[J]. Acta Materialia, 2009, 57(4): 980-992. doi: 10.1016/j.actamat.2008.10.024
    [19]
    KRISHNAMURTHY R, SROLOVITZ D J. Sintering and microstructure evolution in columnar thermal barrier coatings[J]. Acta Materialia, 2009, 57(4): 1035-1048. doi: 10.1016/j.actamat.2008.10.053
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